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Record the weight of the dry, recrystallized acetaminophen and the % recovery from recrystallization (eg; if you obtain g recrystallized product after starting with g crude product you have / x = 75% recovery.
Record the percent theoretical yield of dry recrystallized product.
The experimental procedure used for this experiment was outlined in the CHEM L lab manual, Experiment #1, Synthesis of Acetaminophen, pages. () Experiment #4 1 Synthesis of Acetaminophen and Analysis of Some Common Analgesics Background In this experiment, p-acetamidophenol (acetaminophen) will be prepared from p- aminophenol by reaction with acetic anhydride.
Weigh out g of p-aminophenol and transfer it into a mL Erlenmeyer flask.
(Avoid contact with skin. You may wish to wear gloves.) Add 25 mL of water. Microsoft Word - Synthesis of Aspirin and usagiftsshops.com Author: Administrator. Introduction: Acetaminophen is a commonly used analgesic, which is essentially just a medicine that relieves pain (Prescott, ).Acetaminophen is created by synthesizing p-Aminophenol with Acetic anhydride.
This reaction occurs when the amine group of the p-aminophenol is acetylated by the acetic anhydride. The resultant is an amide functional group (Ellis, ). Insulin is a hormone that is produced and stored in the beta cells of the pancreas.
It is secreted in response to elevated blood glucose following a meal and is vital for the transportation and storage of glucose, the body's main source of energy.
Insulin helps transport glucose from the blood to within cells, thus helping regulate blood glucose levels, and has a role in lipid metabolism.Lab 1 synthesis of acetaminophen